Triethylamine → 2-Ethanoylaminododecyl octadec-9-enoate

HRID 374863Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 374863
[C:1]([NH:4][CH:5]([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH2:6][OH:7])(=[O:3])[CH3:2].C(N(CC)CC)C.[C:25](Cl)(=[O:43])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32]/[CH:33]=[CH:34]\[CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH3:42]>ClCCl>[C:25]([O:7][CH2:6][CH:5]([NH:4][C:1](=[O:3])[CH3:2])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])(=[O:43])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH:33]=[CH:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH3:42]

Komponenten

5

Edukt 3

HCID 8471TriethylamineHCID 5364783Oleoyl chlorideHCID 15076672HCID 15076672, Verbindung

Produkt 1

HCID 545342222-Ethanoylaminododecyl octadec-9-enoateAusbeute 82,8 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

To a solution of 2.43 g of 2-ethanoylaminododecanol, 3 g of triethylamine in 50 ml of dichloromethane is added 3.2 g of oleoyl chloride. The reaction mixture is worked up as under Example 9 to give 4.2 g of product.

Quellen und Nachweise

ORD-Eintrag
ord-930c7ce9323a4dae801e376d8c26b843
Quelldatensatz
uspto-grants-1996_01
Patentnummer
US05482965

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