HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → N-(hydroxymethyl)acetamide acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | Formicin | HCID 69365 | — |
| Katalysator | Pyridine | HCID 1049 | — |
| Produkt | N-(hydroxymethyl)acetamide acetate | HCID 86745977 | 900% |
Reaktionsschritte
Acetic anhydride (25 g) and pyridine (10 drops) is added to N-(hydroxymethyl)acetamide (9 g, 0.1 mol). The reaction mixture is stirred overnight at room temperature, concentrated in vacuo and chased with xylene to give the title product as an oil (11.9 g, 0.9 mol) which is identified by 1HNMR spectral analysis.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05484807 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-452be2e369b949f39458cfbb65e5b732 |
| Quellennotiz | uspto-grants-1996_01 |