HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(2,4-Dimethoxyphenyl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(2,4-Dimethoxyphenyl)prop-2-enoic acid | HCID 85636 | — |
| Edukt | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Produkt | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)- | HCID 6448853 | 20% |
Reaktionsschritte
Substantially the same procedure as in Example 7 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3diethyluracil and 2.89 g (13.9 mmol) of 2,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/ethanol to give 0.92 g (yield 20%) of Compound 68 as yellow crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05484920 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-5849e0e2147e4075a013afb0933396a6 |
| Quellennotiz | uspto-grants-1996_01 |