Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 375298Erstellt: 24. Oktober 2026

3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)-

https://huagongshe.com/de/reaction/375298

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-(1,3-Benzodioxol-5-yl)prop-2-enoic acidHCID 16917—
Edukt5,6-Diamino-1,3-diethyluracilHCID 4572133—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)-HCID 644886338%

Reaktionsschritte

Substantially the same procedure as in Example 7 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.33 g (12.1 mmol) of 3,4methylenedioxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 1.34 g (yield 38%) of Compound 78 as a yellowish green powder.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05484920
Quelldatensatzuspto-grants-1996_01
ORD IDord-95ac9307624d4b3bab7f5b9483857a51
Quellennotizuspto-grants-1996_01