HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid | HCID 16917 | — |
| Edukt | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Produkt | 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)- | HCID 6448863 | 38% |
Reaktionsschritte
Substantially the same procedure as in Example 7 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.33 g (12.1 mmol) of 3,4methylenedioxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 1.34 g (yield 38%) of Compound 78 as a yellowish green powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05484920 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-95ac9307624d4b3bab7f5b9483857a51 |
| Quellennotiz | uspto-grants-1996_01 |