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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 375300Erstellt: 24. Oktober 2026

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/de/reaction/375300

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5,6-Diamino-1,3-dimethyluracilHCID 79501—
Edukt3-(2,3,4-Trimethoxyphenyl)-2-propenoic acidHCID 118400—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-HCID 644875035%

Reaktionsschritte

Substantially the same procedure as in Example 7 was repeated using 5.00 g (29.4 mmol) of 5,6-diamino-1,3-dimethyluracil and 7.71 g (32.4 mmol) of 2,3,4-trimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from isopropanol/water to give 3.78 g (yield 35%) of Compound 82 as an ocher powder.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05484920
Quelldatensatzuspto-grants-1996_01
ORD IDord-7745882e13d44feaacde022f40b4e6aa
Quellennotizuspto-grants-1996_01