HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| Edukt | 3-(2,3,4-Trimethoxyphenyl)-2-propenoic acid | HCID 118400 | — |
| Produkt | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)- | HCID 6448750 | 35% |
Reaktionsschritte
Substantially the same procedure as in Example 7 was repeated using 5.00 g (29.4 mmol) of 5,6-diamino-1,3-dimethyluracil and 7.71 g (32.4 mmol) of 2,3,4-trimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from isopropanol/water to give 3.78 g (yield 35%) of Compound 82 as an ocher powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05484920 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-7745882e13d44feaacde022f40b4e6aa |
| Quellennotiz | uspto-grants-1996_01 |