HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 3-(3-Fluorophenyl)propanoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| Produkt | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
Reaktionsschritte
A solution of 3-fluorohydrocinnamic acid (28 g) in thionyl chloride (90 ml) was heated at reflux for 3 hours. 3-Fluorohydrocinnamoyl chloride (27 g) was isolated by distillation (150°-110° C. @ ca 20 mm.Hg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05486541 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-66e7a4465c454ece8d230e1ae0a91cbd |
| Quellennotiz | uspto-grants-1996_01 |