Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 376467Erstellt: 25. Oktober 2026

4-(2-Phenylethenyl)pyridine → N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide

https://huagongshe.com/reaction/376467

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-(2-Phenylethenyl)pyridineHCID 101576—
Edukt1,3-Dioxane, 2-(2-bromoethyl)-HCID 520656—
LösungsmittelEthyl AcetateHCID 8857—
ProduktN-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromideHCID 7026057690,5%

Reaktionsschritte

4-styrylpyridine (1.81 g) and 2-(2-bromoethyl) 1,3-dioxane (1.95 g) were stirred and refluxed in ethylacetate (15 ml) solution for 15 hours. After cooling of the reaction mixture creamy crystals were separated by filtration, washed with ethyl ether and dried to give 3.4 g of N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06020436
Quelldatensatzuspto-grants-2000_02
ORD IDord-2142058c6b9d4f65bbba617e9cf0cfd1
Quellennotizuspto-grants-2000_02