HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(2-Phenylethenyl)pyridine → N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(2-Phenylethenyl)pyridine | HCID 101576 | — |
| Edukt | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide | HCID 70260576 | 90,5% |
Reaktionsschritte
4-styrylpyridine (1.81 g) and 2-(2-bromoethyl) 1,3-dioxane (1.95 g) were stirred and refluxed in ethylacetate (15 ml) solution for 15 hours. After cooling of the reaction mixture creamy crystals were separated by filtration, washed with ethyl ether and dried to give 3.4 g of N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06020436 |
| Quelldatensatz | uspto-grants-2000_02 |
| ORD ID | ord-2142058c6b9d4f65bbba617e9cf0cfd1 |
| Quellennotiz | uspto-grants-2000_02 |