Ammonia → 5-Imino-1,3,3-trimethylcyclohexane-1-carbonitrile

HRID 377064

Reaktionsgleichung

[C:1]([C:3]1([CH3:12])[CH2:8][C:7]([CH3:10])([CH3:9])[CH2:6][C:5](=O)[CH2:4]1)#[N:2].[NH3:13]>>[C:1]([C:3]1([CH3:12])[CH2:8][C:7]([CH3:10])([CH3:9])[CH2:6][C:5](=[NH:13])[CH2:4]1)#[N:2]

Komponenten

Edukt 2

HCID 222Ammonia

HCID 990683-Cyano-3,5,5-trimethylcyclohexanone

Produkt 1

HCID 117449815-Imino-1,3,3-trimethylcyclohexane-1-carbonitrile

Versuchsvorschrift

imination of 3-cyano-3,5,5-trimethylcyclohexanone with ammonia in the presence of an imination catalyst at temperatures ranging from 20° to 150° C. and pressures ranging from 1.5 to 30 MPa to form 3-cyano-3,5,5-trimethylcyclohexanone imine followed by

Aufarbeitung

customranging from 20° to 150° C.

Quellen und Nachweise

ORD-Eintrag: ord-f80d41fcd0904d42aa5bc29dde0426c6
Quelldatensatz: uspto-grants-2000_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06022999

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