1-(3,5-Dimethoxyphenyl)piperazine → 1-[(5-Acetyl-2-methoxy-4-methylphenyl)aminothiocarbonyl]-4-(3,5-dimethoxyphenyl)piperazine

HRID 377932Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 377932
[C:1]([C:4]1[C:5]([CH3:22])=[CH:6][C:7]([O:20][CH3:21])=[C:8]([NH:10][C:11](=[S:19])OC2C=CC=CC=2)[CH:9]=1)(=[O:3])[CH3:2].[CH3:23][O:24][C:25]1[CH:26]=[C:27]([N:33]2[CH2:38][CH2:37][NH:36][CH2:35][CH2:34]2)[CH:28]=[C:29]([O:31][CH3:32])[CH:30]=1>>[C:1]([C:4]1[C:5]([CH3:22])=[CH:6][C:7]([O:20][CH3:21])=[C:8]([NH:10][C:11]([N:36]2[CH2:35][CH2:34][N:33]([C:27]3[CH:26]=[C:25]([O:24][CH3:23])[CH:30]=[C:29]([O:31][CH3:32])[CH:28]=3)[CH2:38][CH2:37]2)=[S:19])[CH:9]=1)(=[O:3])[CH3:2]

Komponenten

3

Edukt 2

HCID 27362051-(3,5-Dimethoxyphenyl)piperazineHCID 53853945Phenyl N-(5-acetyl-2-methoxy-4-methylphenyl)thiocarbamate

Produkt 1

HCID 537148331-[(5-Acetyl-2-methoxy-4-methylphenyl)aminothiocarbonyl]-4-(3,5-dimethoxyphenyl)piperazineAusbeute 82 %

Versuchsvorschrift

Phenyl N-(5-acetyl-2-methoxy-4-methylphenyl)thiocarbamate and 1-(3,5-dimethoxyphenyl)piperazine were reacted by the same way with the example 197 to obtain the titled compound.

Quellen und Nachweise

ORD-Eintrag
ord-1322f69e22cb4c11b0554f691170baa7
Quelldatensatz
uspto-grants-2000_02
Patentnummer
US06028195

Notizen zur Reaktion

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