1-(3,5-Dichlorophenyl)piperazine → 1-[(5-Acetyl-2-methoxy-4-methylphenyl)aminothiocarbonyl]-4-(3,5-dichlorophenyl)piperazine

HRID 377933

Reaktionsgleichung

Reaktionsgleichung von HRID 377933
[C:1]([C:4]1[C:5]([CH3:22])=[CH:6][C:7]([O:20][CH3:21])=[C:8]([NH:10][C:11](=[S:19])OC2C=CC=CC=2)[CH:9]=1)(=[O:3])[CH3:2].[Cl:23][C:24]1[CH:25]=[C:26]([N:31]2[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]2)[CH:27]=[C:28]([Cl:30])[CH:29]=1>>[C:1]([C:4]1[C:5]([CH3:22])=[CH:6][C:7]([O:20][CH3:21])=[C:8]([NH:10][C:11]([N:34]2[CH2:33][CH2:32][N:31]([C:26]3[CH:25]=[C:24]([Cl:23])[CH:29]=[C:28]([Cl:30])[CH:27]=3)[CH2:36][CH2:35]2)=[S:19])[CH:9]=1)(=[O:3])[CH3:2]

Komponenten

3

Edukt 2

HCID 27360671-(3,5-Dichlorophenyl)piperazineHCID 53853945Phenyl N-(5-acetyl-2-methoxy-4-methylphenyl)thiocarbamate

Produkt 1

HCID 538821041-[(5-Acetyl-2-methoxy-4-methylphenyl)aminothiocarbonyl]-4-(3,5-dichlorophenyl)piperazineAusbeute 79 %

Versuchsvorschrift

Phenyl N-(5-acetyl-2-methoxy-4-methylphenyl)thiocarbamate and 1-(3,5-dichlorophenyl)piperazine were reacted by the same way with the example 197 to obtain the titled compound.

Quellen und Nachweise

ORD-Eintrag
ord-1884c4b5c91642b1ba75e194c3b038e8
Quelldatensatz
uspto-grants-2000_02
Patentnummer
US06028195

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