Diethylamine → N,N-Diethyl-2,5-bis(trifluoromethyl)benzamide
Reaktionsgleichung
[F:1][C:2]([F:17])([F:16])[C:3]1[CH:11]=[CH:10][C:9]([C:12]([F:15])([F:14])[F:13])=[CH:8][C:4]=1[C:5](Cl)=[O:6].[CH2:18]([NH:20][CH2:21][CH3:22])[CH3:19]>>[CH2:18]([N:20]([CH2:21][CH3:22])[C:5](=[O:6])[C:4]1[CH:8]=[C:9]([C:12]([F:15])([F:14])[F:13])[CH:10]=[CH:11][C:3]=1[C:2]([F:17])([F:16])[F:1])[CH3:19]Komponenten
3
Versuchsvorschrift
N,N-Diethyl-2,5-bis(trifluoromethyl)benzamide was prepared from 2,5-bis(trifluoromethyl)benzoyl chloride and diethylamine according to General Method E1. The desired intermediate was isolated in quantitative yield (11.3 g) without additional purification.
Quellen und Nachweise
- ORD-Eintrag
- ord-eef626febdf54792931c908dff72677f
- Quelldatensatz
- uspto-grants-2000_02
- Patentnummer
- US06028101
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