HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole → HCID 178488922, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole | HCID 178488923 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178488922 | HCID 178488922 | 102,4% |
Reaktionsschritte
2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole (10 g) is mixed with EtOH (80 ml) and 5% Pd—C (wet, 2 g). The mixture is shaken under hydrogen at 50 psi for 45 min. then filtered through Celite. The filtrate is evaporated under reduced pressure to yield 2-(4-methoxyphenyl)-4-(2-aminophenyl)imidazole (9.2 g) as a brown solid which is used in the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06297252B1 |
| Quelldatensatz | uspto-grants-2001_10 |
| ORD ID | ord-9236ac423ae6432dac0f2c4e14c88801 |
| Quellennotiz | uspto-grants-2001_10 |