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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 378900Erstellt: 25. Oktober 2026

2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole → HCID 178488922, Verbindung

https://huagongshe.com/reaction/378900

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazoleHCID 178488923—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
ProduktHCID 178488922HCID 178488922102,4%

Reaktionsschritte

2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole (10 g) is mixed with EtOH (80 ml) and 5% Pd—C (wet, 2 g). The mixture is shaken under hydrogen at 50 psi for 45 min. then filtered through Celite. The filtrate is evaporated under reduced pressure to yield 2-(4-methoxyphenyl)-4-(2-aminophenyl)imidazole (9.2 g) as a brown solid which is used in the next step without further purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06297252B1
Quelldatensatzuspto-grants-2001_10
ORD IDord-9236ac423ae6432dac0f2c4e14c88801
Quellennotizuspto-grants-2001_10