HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-Nitrodiphenylamine | HCID 13271 | — |
| Edukt | Methyl bromoacetate | HCID 60984 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate | HCID 54362794 | — |
Reaktionsschritte
4-Nitro-diphenylamine (Aldrich) is reacted with methyl bromoacetate in the presence of potassium carbonate in DMF at 70° C. to give methyl [(4-nitro-phenyl)-phenyl-amino]-acetate (brown oil). MS: 287 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06297266B1 |
| Quelldatensatz | uspto-grants-2001_10 |
| ORD ID | ord-4befb3919eea43d0a93eef70b3a9de60 |
| Quellennotiz | uspto-grants-2001_10 |