HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Fluorobenzoyl chloride → Ethyl 9-chloro-3-(3-fluorobenzoyl)-1,2,3,6-tetrahydroazepino[4,5-B]indole-5-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Fluorobenzoyl chloride | HCID 74376 | — |
| Edukt | Ethyl 9-chloro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate | HCID 66640154 | — |
| Produkt | Ethyl 9-chloro-3-(3-fluorobenzoyl)-1,2,3,6-tetrahydroazepino[4,5-B]indole-5-carboxylate | HCID 57559114 | — |
Reaktionsschritte
The title compound was prepared in a manner similar to that described in Example 2A by using ethyl 9-chloro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate and 3-fluorobenzoyl chloride; 1H-NMR (CDCl3): δ 10.61 (1H, br s), 8.07 (1H, s), 7.46 (2H, m), 7.28 (4H, m), 7.14 (1H, dd), 4.25 (2H, q), 4.19 (2H, t), 3.21 (2H, t), 1.22 (3H, t); MS (ES): 413 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524704B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-435828ba86f04a34b0cec216d0eaefe0 |
| Quellennotiz | uspto-grants-2013_09 |