3,4-Difluorobenzoyl chloride → HCID 57559105, Verbindung

HRID 37968Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 37968
FC1C=C(C=CC=1F)C(Cl)=O.C[C:13]1(C)[C:26]2[C:25]3[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=3[NH:19][C:18]=2[CH:17]([C:27]([O:29][CH2:30][CH3:31])=[O:28])[CH2:16][NH:15][CH2:14]1>>[CH2:30]([O:29][C:27]([CH:17]1[C:18]2[NH:19][C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][C:25]=3[C:26]=2[CH2:13][CH2:14][NH:15][CH2:16]1)=[O:28])[CH3:31]

Komponenten

3

Edukt 2

HCID 27245193,4-Difluorobenzoyl chlorideHCID 66640319HCID 66640319, Verbindung

Produkt 1

HCID 57559105HCID 57559105, Verbindung

Versuchsvorschrift

In a manner similar to that described in Step B, but using 3,4-difluorobenzoyl chloride and ethyl 1,1-dimethyl-1,2,3,4,5,6-hexahydroazepino[4,5-b]indole-5-carboxylate which was prepared in a similar manner as described in Step A, the following compound was prepared:

Aufarbeitung

  1. customwas prepared in a similar manner
  2. customthe following compound was prepared

Quellen und Nachweise

ORD-Eintrag
ord-797c4af4998b454f91a2c2b79f6f8c14
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08524704B2

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