Acetyl chloride → HCID 18367991, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:12]([C:14]1[C:19]([CH3:20])=[CH:18][CH:17]=[CH:16][N:15]=1)=[O:13].[C:21](Cl)(=[O:23])[CH3:22]>>[C:21]([NH:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:12]([C:14]1[C:19]([CH3:20])=[CH:18][CH:17]=[CH:16][N:15]=1)=[O:13])(=[O:23])[CH3:22]Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure described in Example 19 from 3-amino-6-chloro-2-(3-methylpyridine-2-carbonyl)indole (Example 367) and acetyl chloride. m.p.: 173-175° C. (recrystallized from ethyl acetate)
Aufarbeitung
- customm.p.: 173-175° C. (recrystallized from ethyl acetate)
Quellen und Nachweise
- ORD-Eintrag
- ord-95f60d3679ac471085c9ab868b280b31
- Quelldatensatz
- uspto-grants-2001_10