Isovaleryl chloride → HCID 18367951, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:12]([C:14]1[C:19]([CH3:20])=[CH:18][CH:17]=[CH:16][N:15]=1)=[O:13].[C:21](Cl)(=[O:26])[CH2:22][CH:23]([CH3:25])[CH3:24]>>[Cl:11][C:7]1[CH:6]=[C:5]2[C:10]([C:2]([NH:1][C:21](=[O:26])[CH2:22][CH:23]([CH3:25])[CH3:24])=[C:3]([C:12]([C:14]3[C:19]([CH3:20])=[CH:18][CH:17]=[CH:16][N:15]=3)=[O:13])[NH:4]2)=[CH:9][CH:8]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure described in Example 19 from 3-amino-6-chloro-2-(3-methylpyridine-2-carbonyl)indole (Example 367) and isovaleryl chloride. m.p.: 142-144° C. (recrystallized from ethyl acetate)
Aufarbeitung
- customm.p.: 142-144° C. (recrystallized from ethyl acetate)
Quellen und Nachweise
- ORD-Eintrag
- ord-9e57b61ac9ae4f859e23e731ced6fbcc
- Quelldatensatz
- uspto-grants-2001_10
- DOI