HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dicyclopentadiene → Ethylene/propylene 5-ethylidene-2-norbornene dicyclopentadiene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dicyclopentadiene | HCID 6492 | — |
| Edukt | Ethylidenenorbornene | HCID 27756 | — |
| Edukt | Triisobutylaluminum | HCID 16682931 | — |
| Produkt | Ethylene/propylene 5-ethylidene-2-norbornene dicyclopentadiene | HCID 131722887 | — |
Reaktionsschritte
The procedure in Example 1 was substantially repeated except that the feeding rates of 5-ethylidene-2-norbornene and dicyclopentadiene were 1.00 kg/hour and 0.30 kg/hour, respectively, and-the rates of the catalysts dimethylsilyl (2,3,4,5-tetramethylcyclopentadienyl) (3-tert-butyl-5-methyl-2-phenoxy)titanium dichloride, triphenylmethyl tetrakis(pentafluorophenyl)borate and triisobutyl aluminum were 0.057 g/hour, 1.722 g/hour and 3.300 g/hour, respectively. At a polymerization temperature of 83° C., ethylene/propylene/5-ethylidene-2-norbornene/dicyclopentadiene copolymer was produced at a rate of 2.0 kg/hour. Detailed results are shown in Table 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06300447B1 |
| Quelldatensatz | uspto-grants-2001_10 |
| ORD ID | ord-2d9f45d4f8b3465592e9d93764e2523e |
| Quellennotiz | uspto-grants-2001_10 |