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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 380269Erstellt: 26. Oktober 2026

Trimethylamine → 1,3-Dihydroxy-5-trimethylsiloxyadamantane

https://huagongshe.com/reaction/380269

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrimethylamineHCID 1146—
EduktChlorotrimethylsilaneHCID 6397—
Edukt1,3,5-AdamantanetriolHCID 9899022—
LösungsmittelDichloromethaneHCID 6344—
Produkt1,3-Dihydroxy-5-trimethylsiloxyadamantaneHCID 21930710—

Reaktionsschritte

This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06303266B1
Quelldatensatzuspto-grants-2001_10
ORD IDord-c1f12315975a4e23b078209576811615
Quellennotizuspto-grants-2001_10