HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Tetralone → 1,2-Dihydro-4-methylnaphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Tetralone | HCID 10724 | — |
| Edukt | HCID 178418373 | HCID 178418373 | — |
| Produkt | 1,2-Dihydro-4-methylnaphthalene | HCID 582327 | 68% |
Reaktionsschritte
α-Tetralone was reacted with methylmagnesium iodide as described in J. Org. Chem., 26, 4165 (1961), without isolation of the intermediate 1-methyl-1-tetralol, to give the desired product, after distillation, in 68% yield as a colorless oil, boiling point 55-57° C. at 0.8 mm Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06307085B1 |
| Quelldatensatz | uspto-grants-2001_10 |
| ORD ID | ord-f467ee58ecf64abf885a0a6430418e94 |
| Quellennotiz | uspto-grants-2001_10 |