HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-3-chloropropane → 1-(3-Phenylpropyl)-4-(3-chloropropyl)piperazine dihydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 1-(3-Phenylpropyl)piperazine | HCID 796534 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | 1-(3-Phenylpropyl)-4-(3-chloropropyl)piperazine dihydrochloride | HCID 20153184 | 219,3% |
Reaktionsschritte
The procedure described in Example 17(a) was followed, using 36.0 g of (3-phenylpropyl)piperazine, 25.0 g of potassium hydroxide, 125 ml of dimethyl sulfoxide and 28.0 g of 1-bromo-3-chloropropane, to give 46.0 g (73% of theory) of 1-(3-phenylpropyl)-4-(3-chloropropyl)piperazine dihydrochloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04722926 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-249a67ffce174364b0ae5c54cd4ac01c |
| Quellennotiz | uspto-grants-1988_02 |