Ethylene di(S-thioacetate) → GDMA Methacrylic Acid
Reaktionsgleichung
[CH2:1]([O:8][C:9]([CH2:11][SH:12])=[O:10])[CH2:2][O:3][C:4]([CH2:6][SH:7])=[O:5].C1CCC(O)([C:19]([C:21]2[CH:26]=CC=C[CH:22]=2)=[O:20])CC1>>[CH2:2]([O:3][C:4]([CH2:6][SH:7])=[O:5])[CH2:1][O:8][C:9]([CH2:11][SH:12])=[O:10].[C:19]([OH:3])(=[O:20])[C:21]([CH3:26])=[CH2:22]Komponenten
3
Versuchsvorschrift
GDMA (556.8 g, 5.15 eq.) was weighed into a 2000 ml, three neck, round bottom flask. MAA (442.9 g, 5.15 eq.) and Irgacure 184 (1.5 g) were weighed into a 500 ml addition funnel equipped with a Teflon stop cock.
Quellen und Nachweise
- ORD-Eintrag
- ord-e7bb9e62c4d24caa9cf852baa657d138
- Quelldatensatz
- uspto-grants-2001_10
- Patentnummer
- US06310161B1
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