HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → (2-Acetyl-4-methylpentyl)trimethylammonium Iodide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | 3-((Dimethylamino)methyl)-5-methyl-2-hexanone | HCID 53419039 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | (2-Acetyl-4-methylpentyl)trimethylammonium Iodide | HCID 86641883 | 68,4% |
Reaktionsschritte
Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524733B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-279e4411a2944fb7abb24634632e5481 |
| Quellennotiz | uspto-grants-2013_09 |