Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 38312Erstellt: 24. Oktober 2026

Methyl iodide → (2-Acetyl-4-methylpentyl)trimethylammonium Iodide

https://huagongshe.com/de/reaction/38312

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl iodideHCID 6328—
Edukt3-((Dimethylamino)methyl)-5-methyl-2-hexanoneHCID 53419039—
LösungsmittelEthyl AcetateHCID 8857—
Produkt(2-Acetyl-4-methylpentyl)trimethylammonium IodideHCID 8664188368,4%

Reaktionsschritte

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08524733B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-279e4411a2944fb7abb24634632e5481
Quellennotizuspto-grants-2013_09