Methyl iodide → (2-Acetyl-4-methylpentyl)trimethylammonium Iodide

HRID 38312

Reaktionsgleichung

Reaktionsgleichung von HRID 38312
[I:1][CH3:2].[CH3:3][N:4]([CH2:6][CH:7]([CH2:11][CH:12]([CH3:14])[CH3:13])[C:8](=[O:10])[CH3:9])[CH3:5]>C(OCC)(=O)C>[I-:1].[C:8]([CH:7]([CH2:11][CH:12]([CH3:14])[CH3:13])[CH2:6][N+:4]([CH3:2])([CH3:5])[CH3:3])(=[O:10])[CH3:9]

Komponenten

4

Edukt 2

HCID 6328Methyl iodideHCID 534190393-((Dimethylamino)methyl)-5-methyl-2-hexanone

Produkt 1

HCID 86641883(2-Acetyl-4-methylpentyl)trimethylammonium IodideAusbeute 68,4 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

Aufarbeitung

  1. filtration, and the resulting preciptant was collected by filtration

Quellen und Nachweise

ORD-Eintrag
ord-279e4411a2944fb7abb24634632e5481
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08524733B2

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