N-(2-cyclohexylethyl)-N-propanesulfonylamine → 4-(N-(2-Cyclohexylethyl)-N-propanesulfonylaminomethyl)-2-(2-methylphenyl)benzoic acid methyl ester
Reaktionsgleichung
[CH:1]1([CH2:7][CH2:8][NH:9][S:10]([CH2:13][CH2:14][CH3:15])(=[O:12])=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:16][O:17][C:18](=[O:34])[C:19]1[CH:24]=[CH:23][C:22]([CH2:25]Br)=[CH:21][C:20]=1[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[CH3:33]>>[CH3:16][O:17][C:18](=[O:34])[C:19]1[CH:24]=[CH:23][C:22]([CH2:25][N:9]([CH2:8][CH2:7][CH:1]2[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]2)[S:10]([CH2:13][CH2:14][CH3:15])(=[O:12])=[O:11])=[CH:21][C:20]=1[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[CH3:33]Komponenten
3
Versuchsvorschrift
The desired product was prepared using the method described in Example 1174B starting with N-(2-cyclohexylethyl)-N-propanesulfonylamine, prepared as in Example 1187A, and 4-bromomethyl-2-(2-methylphenyl)benzoic acid methyl ester, prepared as in Example 1178A-D. m/e (ESI) 472 (MH+)
Quellen und Nachweise
- ORD-Eintrag
- ord-415f572931dd466ea484587b8b67b534