HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclohexyl isocyanate → HCID 178418497, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclohexyl isocyanate | HCID 18502 | — |
| Edukt | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol | HCID 13731125 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 178418497 | HCID 178418497 | 170,7% |
Reaktionsschritte
The procedure described in Example 35 was followed, using 1.7 g of cyclohexyl isocyanate, 4.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol and 100 ml of methylene chloride, to give 3.8 g (58% of theory) of N-cyclohexyl-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 262°-267° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04722926 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-a34cebc025d14918a8b53e7fb7577a4a |
| Quellennotiz | uspto-grants-1988_02 |