3-Chloroaniline → 5-[(3-Chlorophenyl)amino]pyrazolo[1,5-a]pyrimidine-3-carboxaldehyde

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

To 5-chloropyrazolo[1,5-a]pyrimidine-3-carbaldehyde (120 mg, 0.66 mmol) in 1.5 ml dioxane was added 3-chloroaniline (35 μL, 3.31 mmol). The mixture was heated in Microwave 10 minutes at 120° C. The solid formed was isolated by filtration and air dried to give 5-(3-chlorophenylamino)pyrazolo[1,5-a]pyrimidine-3-carbaldehyde as orange solid. LCMS (M+1=273)

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