HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hexyl isocyanate → HCID 178418561, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hexyl isocyanate | HCID 75659 | — |
| Edukt | 3-[4-(4-Chlorobenzyl)homopiperazin-1-yl]-propanethiol | HCID 20153174 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 178418561 | HCID 178418561 | 77,6% |
Reaktionsschritte
The procedure described in Example 2 was followed, using 1.3 g of n-hexyl isocyanate, 3.0 g of 3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propanethiol and 75 ml of methylene chloride, to give 1.3 g (33% of theory) of N-(n-hexyl)-S-{3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propyl}thiocarbamate dihydrochloride as a tan powder, M.p. 183°-187° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04722926 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-111c8594f1d44a3f8495a7a4086c6573 |
| Quellennotiz | uspto-grants-1988_02 |