HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 1-Bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2,2,3,3,3-Pentafluoropropyl trifluoromethanesulfonate | HCID 2776019 | — |
| Edukt | 4-Bromo-3-fluorophenol | HCID 2779153 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 1-Bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene | HCID 87443298 | — |
Reaktionsschritte
The title compound was prepared from 4-bromo-3-fluorophenol and 2,2,3,3,3,-pentafluoropropyl triflate with potassium carbonate in acetone at ambient temperature for 18 hours. Kugelrohr distillation provided a colorless oil, b.p. 105-110° C./12 mbar.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08367838B2 |
| Quelldatensatz | uspto-grants-2013_02 |
| ORD ID | ord-7ef815b8595f4da1b115d094560517b9 |
| Quellennotiz | uspto-grants-2013_02 |