HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Diiodobenzene → Rac-[1-(3-chloro-4-methyl-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Diiodobenzene | HCID 12208 | — |
| Edukt | Rac-[(3-chloro-4-methyl-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 87442965 | — |
| Produkt | Rac-[1-(3-chloro-4-methyl-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68410985 | — |
Reaktionsschritte
The title compound was prepared from rac-[(3-chloro-4-methyl-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 4) and 1,4-di-iodobenzene in analogy to Example 1a): MS (ISN): 484.2 (M−H)−.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08367838B2 |
| Quelldatensatz | uspto-grants-2013_02 |
| ORD ID | ord-5e610819da794f64b32c31a975001c06 |
| Quellennotiz | uspto-grants-2013_02 |