(R)-1-[3-Amino-4-(benzyloxy)phenyl]-2-bromoethanol → (R)-1-(3-Amino-4-(benzyloxy)phenyl)-2-azidoethanol

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	(R)-1-[3-Amino-4-(benzyloxy)phenyl]-2-bromoethanol	HCID 11232489	—
Edukt	(R)-5-(2-Azido-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-(benzyloxy)quinolin-2(1H)-one	HCID 58505233	—
Produkt	(R)-1-(3-Amino-4-(benzyloxy)phenyl)-2-azidoethanol	HCID 57516929	—

Reaktionsschritte

The title compound was synthesized in a manner analogous to that described for Intermediate 1, using Intermediate 13 in place of (R)-8-(benzyloxy)-5-[2-bromo-1-[(tert-butyldimethylsilyl)oxy]ethyl]quinolin-2(1H)-one. ES/MS calcd. for C15H17N4O2+ 285.1. found m/z=285 (M+H)+.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08367829B2
Quelldatensatz	uspto-grants-2013_02
ORD ID	ord-ca1fe8518ed244528c31c3a40eed3069
Quellennotiz	uspto-grants-2013_02