Thionyl Chloride → 1093881-63-0

HRID 385888

Reaktionsgleichung

Reaktionsgleichung von HRID 385888
[CH3:1][N:2]1[CH:6]=[C:5]([CH2:7][CH2:8]O)[CH:4]=[N:3]1.S(Cl)([Cl:12])=O>>[Cl:12][CH2:8][CH2:7][C:5]1[CH:4]=[N:3][N:2]([CH3:1])[CH:6]=1

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 170280762-(1-Methyl-1H-pyrazol-4-yl)ethanol

Produkt 1

HCID 595256861093881-63-0

Versuchsvorschrift

To excess thionyl chloride (250 mL) at 0° C. was added 2-(1-methyl-1H-pyrazol-4-yl)ethanol (82 g, 0.651 mol). The reaction mixture was heated to reflux for 15 minutes. The excess thionyl chloride was removed in vacuo and the crude product was purified by recrystallization from EtOH to afford the title compound.

Aufarbeitung

  1. temperatureThe reaction mixture was heated
  2. temperatureto reflux for 15 minutes
  3. customThe excess thionyl chloride was removed in vacuo
  4. customthe crude product was purified by recrystallization from EtOH

Quellen und Nachweise

ORD-Eintrag
ord-8cf3da863bb44cb5b5e5721caf418352
Quelldatensatz
uspto-grants-2013_02
Patentnummer
US08367706B2

Verknüpfte Notizen

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