Thionyl Chloride → HCID 59526066, Verbindung

HRID 386120Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 386120
[CH3:1][C:2](=[N:4][O:5][CH2:6][C:7]([OH:9])=O)[CH3:3].S(Cl)([Cl:12])=O>C1(C)C=CC=CC=1>[CH3:1][C:2](=[N:4][O:5][CH2:6][C:7]([Cl:12])=[O:9])[CH3:3]

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 79344[(2-Propanylideneamino)oxy]acetic acid

Produkt 1

HCID 59526066HCID 59526066, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

To {[(1-methylethylidene)amino]oxy}acetic acid (286 g, 2.18 mol) was added 600 ml of toluene. Thionyl chloride (364 g, 3.06 mol) was added dropwise at room temperature. After the addition was complete, the reaction mixture was heated to reflux for 10 hours. Toluene and thionyl chloride were evaporated under vacuum and the residue was distilled to afford the title compound.

Aufarbeitung

  1. additionAfter the addition
  2. temperaturethe reaction mixture was heated
  3. temperatureto reflux for 10 hours
  4. customToluene and thionyl chloride were evaporated under vacuum
  5. distillationthe residue was distilled

Quellen und Nachweise

ORD-Eintrag
ord-10e3dbd5cef642c3a68a50a65e46166f
Quelldatensatz
uspto-grants-2013_02
Patentnummer
US08367706B2

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