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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 386846Erstellt: 25. Oktober 2026

2,6-Dimethyl-4-pyranone → cis-2,6-dimethyloxan-4-one

https://huagongshe.com/reaction/386846

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,6-Dimethyl-4-pyranoneHCID 13862—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
Produktcis-2,6-dimethyloxan-4-oneHCID 1044171688%

Reaktionsschritte

10 g of 2,6-dimethyl-gamma-pyrone are dissolved in 200 ml of methanol and then 0.8 g of palladium-on-charcoal at 10% is added. The reaction mixture is stirred for 24 hours under 25 atmospheres of hydrogen. The medium is filtered and then the solvent is evaporated off. 8.81 g of cis-2,6-dimethyltetrahydro-pyran-4-one are recovered. Yield=88%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08372879B2
Quelldatensatzuspto-grants-2013_02
ORD IDord-6f65603ea42e4edab860129fe6f3e19a
Quellennotizuspto-grants-2013_02