HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Phenylpiperazine → HCID 25066507, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Phenylpiperazine | HCID 7096 | — |
| Edukt | Diisopropylethylamine | HCID 81531 | — |
| Edukt | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Edukt | 3-(1-tert-butyl-5-(4-chlorophenyl)-1H-pyrazol-3-yl)propanal | HCID 86639921 | — |
| Produkt | HCID 25066507 | HCID 25066507 | — |
Reaktionsschritte
116 mg (89%) of target compound was obtained by using a method same as in Example 1 by using 3-(1-tert-butyl-5-(4-chlorophenyl)-1H-pyrazol-3-yl)propanal (80 mg, 0.275 mmol), 1-phenylpiperazine (0.041 mL, 0.275 mmol), DIPEA (0.072 mL, 0.413 mmol) and NaBH(OAc)3 (175 mg, 0.825 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08372844B2 |
| Quelldatensatz | uspto-grants-2013_02 |
| ORD ID | ord-9bca022f846f4f8f95a4c2bd46b5e5db |
| Quellennotiz | uspto-grants-2013_02 |