HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 389236Erstellt: 25. Oktober 2026
1,4-Dichlorobenzene → 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide
https://huagongshe.com/reaction/389236
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1,4-Dichlorobenzene | HCID 4685 | — |
| Edukt | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| Edukt | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| Produkt | 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide | HCID 68813660 | — |
Reaktionsschritte
To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08378120B2 |
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| Quelldatensatz | uspto-grants-2013_02 |
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| ORD ID | ord-d7d322c6a96a4247a8c483bed3a38135 |
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| Quellennotiz | uspto-grants-2013_02 |
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