HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Piperidine → Phe-Gly
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Piperidine | HCID 8082 | — |
| Edukt | Fmoc-Phe-Gly-OH | HCID 11328236 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Phe-Gly | HCID 6992304 | — |
Reaktionsschritte
Fmoc-protected dipeptide 72 (500 mg, 1.00 mmol) was treated with a 5% v/v solution of piperidine in DMF (5 mL). After stirring for 1 h, the reaction mixture was concentrated to dryness. The crude material was used for the next step without purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524691B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-f2ae1b8090a940d2913985de4b8df854 |
| Quellennotiz | uspto-grants-2013_09 |