HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Piperidine → Glycyl-phenylalanyl-glycine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Piperidine | HCID 8082 | — |
| Edukt | N-Fmoc-glycyl-L-phenylalanyl-glycine | HCID 15222489 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Glycyl-phenylalanyl-glycine | HCID 6992441 | — |
Reaktionsschritte
Fmoc-protected tripeptide 74 (546 mg, 0.98 mmol) was treated with a 5% v/v solution of piperidine in DMF (5 mL). After stirring for 45 min, the reaction mixture was concentrated to dryness. The crude material was used for the next step without purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524691B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-7e66b13904154ebcbe524b75757fe2f1 |
| Quellennotiz | uspto-grants-2013_09 |