2-Phenyl-1-propanol → Diphenylacetyl-carbamic acid (RS)-2-phenyl-propyl ester

HRID 392701

Reaktionsgleichung

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:19]1([CH:25]([CH3:28])[CH2:26][OH:27])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:19]1([CH:25]([CH3:28])[CH2:26][O:27][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Komponenten

Edukt 2

HCID 142952-Phenyl-1-propanol

HCID 11264874Diphenylacetyl isocyanate

Produkt 1

HCID 53881928Diphenylacetyl-carbamic acid (RS)-2-phenyl-propyl ester

Versuchsvorschrift

The title compound, white solid, m.p. 131° C. and MS: m/e=373.5 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and (RS)-2-phenyl-propan-1-ol.

Quellen und Nachweise

ORD-Eintrag: ord-9ade69da4c534383bed2a987a8afda88
Quelldatensatz: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06803381B1

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