HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N,3-trimethyl-4-nitrobenzamide → 4-amino-N,N,3-trimethylbenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N,3-trimethyl-4-nitrobenzamide | HCID 786992 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-amino-N,N,3-trimethylbenzamide | HCID 16781770 | — |
Reaktionsschritte
N,N,3-trimethyl-4-nitrobenzamide (0.6 g, 2.88 mmol) in methanol was hydrogenated using the H-cube apparatus (1.2 mL/min, RT, atmospheric pressure). After 45 minutes the reaction was complete. Removal of the solvent in vacuo gave 4-amino-N,N,3-trimethylbenzamide as a colourless solid (quantitative); MS (ES+) 179.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524902B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-3fa264f9a8bd4375af3bdd364a61e69a |
| Quellennotiz | uspto-grants-2013_09 |