Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrogen Peroxide | HCID 784 | — |
| Edukt | 3-Fluoropyridine-4-carboxylic acid | HCID 345361 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 3-Fluoroisonicotinic acid 1-oxide | HCID 57649637 | — |
Reaktionsschritte
To a solution of 3-fluoroisonicotinic acid (5.0 g, 35.33 mmol) in acetic acid (25 ml) was added hydrogen peroxide (6 ml). The reaction mixture was stirred at 70-80° C. overnight. The solvent was removed to obtain 5.5 g of 3-fluoroisonicotinic acid 1-oxide in quantitative yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08524911B2 |
|---|
| Quelldatensatz | uspto-grants-2013_09 |
|---|
| ORD ID | ord-eefb4f777a6c4d60abf2477d1e1f9e78 |
|---|
| Quellennotiz | uspto-grants-2013_09 |
|---|
