HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 395264Erstellt: 26. Oktober 2026
Hydrogen Bromide → 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol hydrobromide
https://huagongshe.com/reaction/395264
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | 7-Methoxy-2,3,4,5-tetrahydro-1h-3-benzazepine | HCID 13853348 | — |
| Produkt | 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol hydrobromide | HCID 23331391 | — |
Reaktionsschritte
7-Methoxy-2,3,4,5-tetrahydro-1H-3-benzazepine (10 g) in 48% aqueous hydrobromic acid (350 ml) was allowed to stir at 100° C. for 4 h. The mixture was cooled to 20° C. then evaporated to dryness in vacuo to give the title compound (14.5 g) as a brown solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06605607B1 |
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| Quelldatensatz | uspto-grants-2003_08 |
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| ORD ID | ord-06c471aa95454f4dbe946f9057bfaef9 |
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| Quellennotiz | uspto-grants-2003_08 |
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