Tert-butyl 4-((4-bromophenyl)amino)piperidine-1-carboxylate → HCID 22557853, Verbindung

HRID 395541

Reaktionsgleichung

Reaktionsgleichung von HRID 395541
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][CH:9]2[CH2:14][CH2:13][N:12]([C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])[CH2:11][CH2:10]2)=[CH:4][CH:3]=1.Cl[CH2:23][C:24]1[CH:25]=[C:26]([C:30]2[CH:35]=[C:34]([O:36][CH3:37])[C:33]([O:38][CH3:39])=[C:32]([O:40][CH3:41])[CH:31]=2)[CH:27]=[N:28][CH:29]=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]([CH:9]2[CH2:10][CH2:11][N:12]([C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])[CH2:13][CH2:14]2)[CH2:23][C:24]2[CH:25]=[C:26]([C:30]3[CH:35]=[C:34]([O:36][CH3:37])[C:33]([O:38][CH3:39])=[C:32]([O:40][CH3:41])[CH:31]=3)[CH:27]=[N:28][CH:29]=2)=[CH:4][CH:3]=1

Komponenten

3

Edukt 2

HCID 11210451Tert-butyl 4-((4-bromophenyl)amino)piperidine-1-carboxylateHCID 225578743-Chloromethyl-5-(3,4,5-trimethoxyphenyl)pyridine

Produkt 1

HCID 22557853HCID 22557853, Verbindung

Versuchsvorschrift

4-(4-Bromophenyl)amino-1-(tert-butoxycarbonyl)piperidine (711 mg) and 5-chloromethyl-3-(3,4,5-trimethoxyphenyl)pyridine (588 mg) was treated in the same manner as described in Example 9 to give light yellow amorphous of the title compound.

Quellen und Nachweise

ORD-Eintrag
ord-a14af0c7d04949599b56ed39e985b41b
Quelldatensatz
uspto-grants-2003_08
Patentnummer
US06605620B1

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