3-Furaldehyde → HCID 21352698, Verbindung

Reaktionsgleichung

[CH3:1][O:2][C:3]1[CH:26]=[CH:25][C:6]([C:7]([NH:9][C:10]2[C:11]([NH:16][C:17]([CH:19]3[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]3)=[O:18])=[CH:12][CH:13]=[CH:14][CH:15]=2)=[O:8])=[CH:5][CH:4]=1.[O:27]1[CH:31]=[CH:30][C:29]([CH:32]=O)=[CH:28]1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([NH:9][C:10]2[C:11]([NH:16][C:17]([CH:19]3[CH2:20][CH2:21][N:22]([CH2:32][C:29]4[CH:30]=[CH:31][O:27][CH:28]=4)[CH2:23][CH2:24]3)=[O:18])=[CH:12][CH:13]=[CH:14][CH:15]=2)=[O:8])=[CH:25][CH:26]=1

Komponenten

Edukt 2

HCID 103513-Furaldehyde

HCID 53635745HCID 53635745, Verbindung

Produkt 1

HCID 21352698HCID 21352698, Verbindung

Versuchsvorschrift

Using the general procedure described in Example 3, N1-(4-methoxybenzoyl)-N2-(piperidin-4-ylcarbonyl)-1,2-benzenediamine (0.045 mmol) was reacted with 3-furaldehyde to provide 19 mg of the title product as the free base. Treatment with hydrochloric acid and concentration in vacuo yielded the salt of the title compound.

Quellen und Nachweise

ORD-Eintrag: ord-768d11340343438384610c3cb74d5b63
Quelldatensatz: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06605626B2

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