2-Acetyl-4-[1-(tert-butyldimethylsilyloxy)ethyl]pyridine → 2-Bromoacety-4-[1-(tert-butyldimethylsilyloxy)ethyl]pyridine
Reaktionsgleichung
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[C:9]([CH2:11][O:12][Si:13]([C:16]([CH3:19])([CH3:18])[CH3:17])([CH3:15])[CH3:14])[CH:8]=[CH:7][N:6]=1)=[O:4].[C:20](C1C=C(C(O[Si](C(C)(C)C)(C)C)C)C=CN=1)(=O)C>>[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[C:9]([CH:11]([O:12][Si:13]([C:16]([CH3:19])([CH3:18])[CH3:17])([CH3:14])[CH3:15])[CH3:20])[CH:8]=[CH:7][N:6]=1)=[O:4]Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure for preparing 2-bromoacetyl-4-(tert-butyldimethylsilyloxymethyl)pyridine described in Example 95 from 2-acetyl-4-[1-(tert-butyldimethylsilyloxy)ethyl]pyridine.
Quellen und Nachweise
- ORD-Eintrag
- ord-67dfd99d90654d4fbf544907ba96f2ca
- Quelldatensatz
- uspto-grants-2003_08
- Patentnummer
- US06608070B1
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