HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glycolic Acid → 2-(Hydroxymethyl)-Alpha,Alpha-dimethyl-1H-imidazo[4,5-c]quinoline-1-ethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glycolic Acid | HCID 757 | — |
| Edukt | 1-((3-Aminoquinolin-4-yl)amino)-2-methylpropan-2-ol | HCID 14986941 | — |
| Produkt | 2-(Hydroxymethyl)-Alpha,Alpha-dimethyl-1H-imidazo[4,5-c]quinoline-1-ethanol | HCID 22672658 | — |
Reaktionsschritte
Using the general method of Example 24, 3-amino-4-(2-hydroxy-2-methylpropylamino)quinoline (45 g, 0.19 mol) was reacted with glycolic acid to provide 35.7 g of the desired product as a tan solid. The structure was confirmed by nuclear magnetic resonance spectroscopy.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06608201B2 |
| Quelldatensatz | uspto-grants-2003_08 |
| ORD ID | ord-1e02acccf44943218c679b2c49b52e4d |
| Quellennotiz | uspto-grants-2003_08 |