HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → HCID 23445018, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Ethyl orthoformate | HCID 31214 | — |
| Edukt | Ethyl nitroacetate | HCID 69379 | — |
| Edukt | 3-Amino-5-fluorobenzotrifluoride | HCID 2735913 | — |
| Katalysator | Iron | HCID 23925 | — |
| Produkt | HCID 23445018 | HCID 23445018 | — |
Reaktionsschritte
Following the general method described in example 234, 3-fluoro-5-trifluoromethylaniline was reacted with triethyl orthoformate, ethyl nitroacetate and acetic acid followed by treatment with triethyl orthoformate, iron and acetic acid and subsequent alkaline hydrolysis. The title compound was obtained as a white crystalline solid. Mp.>250° C. (H2O/dioxane), MS: m/e=273 (M−H−).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06610723B2 |
| Quelldatensatz | uspto-grants-2003_08 |
| ORD ID | ord-b147aa1cff6e43aeaab32b572cddd72d |
| Quellennotiz | uspto-grants-2003_08 |