HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
{[4-(Methylsulfanyl)phenyl]methyl}(triphenyl)phosphanium chloride → HCID 12652959, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | {[4-(Methylsulfanyl)phenyl]methyl}(triphenyl)phosphanium chloride | HCID 18969794 | — |
| Katalysator | Benzyltriphenylphosphonium chloride | HCID 70671 | — |
| Produkt | HCID 12652959 | HCID 12652959 | — |
Reaktionsschritte
Following the procedure as describe in method 1, but sustituting 4-methylthiobenzyltriphenylphosphonium chloride for benzyltriphenylphosphonium chloride, the desired residue was purified by flash chromatography (silica gel; hexane/EtOAc (90:10)) and recrystallisation from hexane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05817700 |
| Quelldatensatz | uspto-grants-1998_10 |
| ORD ID | ord-92dd2f6185b44d6eb92558a7134d09c5 |
| Quellennotiz | uspto-grants-1998_10 |