HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 399189Erstellt: 25. Oktober 2026
1-Naphthalenecarboxamide → 2-Naphthalenecarbonitrile
https://huagongshe.com/reaction/399189
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
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| Edukt | 1-Naphthalenecarboxamide | HCID 75244 | — |
| Edukt | Sulfur trioxide triethylamine complex | HCID 222301 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | 2-Naphthalenecarbonitrile | HCID 11944 | 91% |
Reaktionsschritte
A suspension of 10 mmol of naphthalenecarboxamide and 25 mmol of triethylamine-sulphur trioxide in 30 ml of triethylamine was stirred at 89° C. for 2 hours. The working up was effected as described under Example 1a). Yield: 91% of theory.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05817827 |
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| Quelldatensatz | uspto-grants-1998_10 |
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| ORD ID | ord-78c48b0b29fa4e708da4076fc22aa64e |
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| Quellennotiz | uspto-grants-1998_10 |
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