HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetyl chloride → Methyl 3-(3-bromophenyl)prop-2-enoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Methyl 3-(3-bromophenyl)prop-2-enoate | HCID 610698 | — |
Reaktionsschritte
To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05827868 |
| Quelldatensatz | uspto-grants-1998_10 |
| ORD ID | ord-f8d184a5c3014a92bc4fb77c554723dc |
| Quellennotiz | uspto-grants-1998_10 |